(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

Base Information

Chemical Name:(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine
CAS No.:198017-85-5
Molecular Formula:C₁₉H₁₇ClN₄
Molecular Weight:336.824
Hs Code.:

Synonyms:(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

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Chemical Property of (4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

Chemical Property:

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Technology Process of (4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

There total 4 articles about (4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1-(4-Chloro-phenyl)-3-(1-{[1-cyclopropyl-1-phenyl-meth-(Z)-ylidene]-hydrazono}-ethyl)-urea

: 198017-85-5
(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

Guidance literature:: With tetrachloromethane; triethylamine; triphenylphosphine; In dichloromethane; for 3h; Heating;
DOI:10.1002/jhet.5570340435

Reference yield:

: 3481-02-5
cyclopropyl phenyl ketone

: 198017-85-5
(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / hydrazine monohydrate / 3 h / Heating

2: 90 percent / methanol / 0.17 h / Heating

3: 86 percent / CH₂Cl₂ / 0.33 h / Ambient temperature

4: 68 percent / Ph₃P, CCl₄, Et₃N / CH₂Cl₂ / 3 h / Heating

With tetrachloromethane; hydrazine hydrate; triethylamine; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1002/jhet.5570340435

Reference yield:

: cyclopropyl phenyl ketone hydrazone

: 198017-85-5
(4-Chloro-phenyl)-[2-(cyclopropylidene-phenyl-methyl)-5-methyl-2H-[1,2,4]triazol-3-yl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / methanol / 0.17 h / Heating

2: 86 percent / CH₂Cl₂ / 0.33 h / Ambient temperature

3: 68 percent / Ph₃P, CCl₄, Et₃N / CH₂Cl₂ / 3 h / Heating

With tetrachloromethane; triethylamine; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1002/jhet.5570340435