3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

Base Information

Chemical Name:3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane
CAS No.:136213-24-6
Molecular Formula:C₃₀H₅₀N₂Si₃
Molecular Weight:522.997
Hs Code.:

Synonyms:3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

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Technology Process of 3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

There total 2 articles about 3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 136213-25-7
3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,5,5-hexamethyl-2,4,5-trisilahexane

: 114533-51-6
2,2,4,4,6,6-hexamethyl-3,5-bis(2,6-dimethylphenylimino)-2,4,6-trisilaheptane

: 136213-24-6
3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

Guidance literature:: With palladium diacetate; In toluene; for 20h; Title compound not separated from byproducts; Heating;
DOI:10.1021/ja00023a043

Reference yield:

: 2008-61-9
2,6-diisopropylphenylisocyanide

: 136213-24-6
3-<(2,6-diisopropylphenyl)imino>-2,2,4,4,6,6-hexamethyl-5-(2,6-xylylimino)-2,4,6-trisilaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / palladium(II) acetate / toluene / 4 h / Heating

2: 43 percent / palladium(II) acetate / toluene / 20 h / Heating

With palladium diacetate; In toluene;
DOI:10.1021/ja00023a043