(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

Base Information

Chemical Name:(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate
CAS No.:1620878-58-1
Molecular Formula:C₁₆H₁₃Cl₂N₃O₃S₂
Molecular Weight:430.336
Hs Code.:

Synonyms:(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

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Technology Process of (E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

There total 4 articles about (E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 58291-89-7
1,3-dichloro-2-(4-methanesulfonylphenoxy)-5-aminobenzene

: 10191-60-3
dimethyl N-cyanodithioiminocarbonate

: 1620878-58-1
(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

Guidance literature:: With pyridine; for 3h; Reflux;

Reference yield:

: 3107-19-5
3,5-dichloro-4-fluoro-nitrobenzene

: 1620878-58-1
(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 110 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 2585.81 Torr

3: pyridine / 3 h / Reflux

With pyridine; palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 58291-68-2
1,3-dichloro-2-(4-methanesulfonylphenoxy)-5-nitrobenzene

: 1620878-58-1
(E)-methyl N'-cyano-N-(3,5-dichloro-4-(4-(methylsulfonyl)phenoxy)phenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 2585.81 Torr

2: pyridine / 3 h / Reflux

With pyridine; palladium 10% on activated carbon; hydrogen; In ethyl acetate;