Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

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Chemical Name:Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester
CAS No.:1205552-21-1
Molecular Formula:C₃₄H₄₃Cl₂N₃O₃
Molecular Weight:612.64
Hs Code.:

Synonyms:Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

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Chemical Property of Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

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Technology Process of Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

There total 2 articles about Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: biphenyl-2-yl-carbamic acid 1-(9-amino-nonyl)-piperidin-4-yl ester dihydrochloride salt

: 56962-13-1
2,4-dichloro-3-hydroxybenzaldehyde

: 1205552-21-1
Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

Guidance literature:: biphenyl-2-yl-carbamic acid 1-(9-amino-nonyl)-piperidin-4-yl ester dihydrochloride salt; 2,4-dichloro-3-hydroxybenzaldehyde; With acetic acid; sodium sulfate; triethylamine; In ethanol; at 20 ℃; for 1h; Inert atmosphere;

With ethanol; sodium cyanoborohydride; at 20 ℃; for 18h; Product distribution / selectivity; Inert atmosphere;

Reference yield: 46.0%

: 743460-14-2
biphenyl-2-yl-carbamic acid 1-(9-amino-nonyl)-piperidin-4-yl ester

: 56962-13-1
2,4-dichloro-3-hydroxybenzaldehyde

: 1205552-21-1
Biphenyl-2-yl-carbamic acid 1-[9-(2,4-dichloro-3-hydroxy-benzylamino)-nonyl]-piperidin-4-yl ester

Guidance literature:: biphenyl-2-yl-carbamic acid 1-(9-amino-nonyl)-piperidin-4-yl ester; 2,4-dichloro-3-hydroxybenzaldehyde; With titanium(IV) isopropylate; In ethanol; at 20 ℃; for 18h;

With sodium tetrahydroborate; ethanol; at 0 - 20 ℃; Product distribution / selectivity;