methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

Base Information

Chemical Name:methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate
CAS No.:1182222-04-3
Molecular Formula:C₁₉H₃₀O₇
Molecular Weight:370.443
Hs Code.:

Synonyms:methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

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Chemical Property of methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

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Technology Process of methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

There total 3 articles about methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1182222-31-6
methyl 2,6-bis(methoxymethoxy)-4-(3-pentyloxiran-2-yl)benzoate

: 1182222-04-3
methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

Guidance literature:: With 5% Pd/CaCO3; hydrogen; In methanol; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ja905387r

Reference yield:

: 3147-39-5
methyl 2,4,6-trihydroxybenzoate

: 1182222-04-3
methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: lutidine / dichloromethane / 16 h / 0 °C / Inert atmosphere

2: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 2.5 h / Inert atmosphere; Reflux

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

5: Lindlar's catalyst; hydrogen / methanol / 20 h / 20 °C / 760.05 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; Lindlar's catalyst; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2018.01.021

Reference yield:

: C₁₉H₂₈O₆

: 1182222-04-3
methyl 4-(2-hydroxyheptyl)-2,6-bis(methoxymethoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

2: Lindlar's catalyst; hydrogen / methanol / 20 h / 20 °C / 760.05 Torr

With Lindlar's catalyst; hydrogen; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.tet.2018.01.021