(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

Base Information

Chemical Name:(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)
CAS No.:60294-99-7
Molecular Formula:C₄₂H₃₉NiP₃S₂
Molecular Weight:759.515
Hs Code.:

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Ni(CS<sub>2</sub>)

Synonyms:(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

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Chemical Property of (CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

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Technology Process of (CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

There total 5 articles about (CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 83561-95-9
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CSMe)]BPh₄

: 60294-99-7
(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

Guidance literature:: With NaBH₄; In ethanol; acetone; (N2); soln. of NaBH4 in EtOH added dropwise to Ni complex suspn. in acetone; EtOH added; elem. anal.;

Reference yield: 70.0%

: 83561-99-3
[(1,1,1-tris((diphenylphosphino)methyl)ethane)Ni(S₂CNEt₂)]BPh₄

: 60294-99-7
(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

: 83562-00-9
(CH₃C(CH₂P(C₆H₅)2)3)Ni(S₂CS)

Guidance literature:: With NaBH₄; CS₂; In ethanol; acetone; soln. of Ni-complex in acetone was treated with NaBH4 in EtOH, CS2 was added, BuOH was added;

Reference yield:

: 83562-00-9
(CH₃C(CH₂P(C₆H₅)2)3)Ni(S₂CS)

: 60294-99-7
(CH₃C(CH₂P(C₆H₅)2)3)Ni(CS₂)

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; dichloromethane

2: dichloromethane

3: NaBH₄; CS₂ / ethanol; acetone

With NaBH₄; CS₂; In ethanol; dichloromethane; acetone;