2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

Base Information

Chemical Name:2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole
CAS No.:1032989-77-7
Molecular Formula:C₃₈H₆₁NO₇S₂Si₂
Molecular Weight:764.208
Hs Code.:

Synonyms:2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

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Chemical Property of 2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

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Technology Process of 2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

There total 14 articles about 2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1032989-99-3
C₃₈H₆₁NO₅S₂Si₂

: 1032989-77-7
2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; for 16h; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield:

: 1032989-86-8
C₃₁H₅₈O₆Si₂

: 1032989-77-7
2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 16 h / Inert atmosphere

With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1039/c2ob25100k

Reference yield:

: 1032989-85-7
C₃₂H₄₈O₆Si

: 1032989-77-7
2-((2R,3S,4R,5S,6S)-6-methoxy-5-(4-methoxybenzyloxy)-2-methyl-3,4-bis(triethylsilyloxy)non-8-enylsulfonyl)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / methanol / 1 h / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 0 °C / Inert atmosphere

3: pyridine; pyridine hydrofluoride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

5: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 16 h / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; hexaammonium heptamolybdate tetrahydrate; pyridine hydrofluoride; dihydrogen peroxide; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1039/c2ob25100k