P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

Base Information

Chemical Name:P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester
CAS No.:486429-67-8
Molecular Formula:C₁₇H₂₃PSSeSi
Molecular Weight:397.455
Hs Code.:

P,P-diphenylphosphinoselenothioic acid S<sub>0</sub>[2-(trimethylsilyl)ethyl] ester

Synonyms:P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

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Chemical Property of P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

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Technology Process of P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

There total 4 articles about P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: lithium 2-(trimethylsilyl)ethanethiolate

: 486429-67-8
P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

Guidance literature:: chloro-diphenylphosphine; With selenium; In tetrahydrofuran;

lithium 2-(trimethylsilyl)ethanethiolate; In tetrahydrofuran; at -78 - 20 ℃; for 2h;
DOI:10.1246/cl.2002.914

Reference yield: 90.0%

: 18143-30-1
2-trimethylsilylethanethiol

: 55249-23-5
diphenylselenophosphinic chloride

: 486429-67-8
P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jo050576c

Reference yield:

: 754-05-2
ethenyltrimethylsilane

: 486429-67-8
P,P-diphenylphosphinoselenothioic acid S₀[2-(trimethylsilyl)ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 23 / 1 h / Heating

2: 78 percent / EtONa / tetrahydrofuran / 12 h / 20 °C

3: 90 percent / tetrahydrofuran / 1 h / 0 °C

With sodium ethanolate; 23; In tetrahydrofuran;
DOI:10.1021/jo050576c