2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine
CAS No.:77489-38-4
Molecular Formula:C₃₃H₃₈N₂O₁₄
Molecular Weight:686.67
Hs Code.:

2,3,4,6-tetra-O-acetyl-1-N-<benzyl N-(benzyloxy)carbonyl-L-aspart-4-oyl>-β-D-glucopyranosylamine

Synonyms:2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

Chemical Property:

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Technology Process of 2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

There total 7 articles about 2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4779-31-1
Z-Asp-OBn

: 14152-97-7
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate

: 77489-38-4
2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

Guidance literature:: triethylamine; In toluene; for 72h; Ambient temperature;
DOI:10.1016/S0008-6215(00)84671-6

Reference yield:

: 4451-36-9
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl chloride

: 77489-38-4
2,3,4,6-tetra-O-acetyl-1-N--β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaN₃ / hexamethylphosphoric acid triamide / 4 h / 20 °C

2: H₂; Et₃N / Lindlar's catalyst / tetrahydrofuran; methanol / 16 h / 1520 Torr

3: HOBt; DCC / CH₂Cl₂ / 13 h / 0 - 20 °C

With sodium azide; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; Lindlar's catalyst; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; 1: Substitution / 2: Catalytic hydrogenation / 3: Acylation;
DOI:10.1515/znb-1999-0519