methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:136824-11-8
Molecular Formula:C₅₅H₆₀O₁₁
Molecular Weight:897.075
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 21 articles about methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 20672-66-6
3,4,6-tri-O-benzyl-D-mannopyranose

: 76679-47-5
methyl-2,3,4-tri-O-benzyl-6-O-trifluoromethanesulfonyl-α-D-glucopyranoside

: 136824-11-8
methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 10-hydroxy-4a,10a-dihydrobenzo[b][1,4]benzoxaborinine; In acetonitrile; at 20 ℃; for 24h; Reagent/catalyst; stereoselective reaction; Molecular sieve;
DOI:10.1021/acs.orglett.8b03823

Reference yield: 99.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 74372-90-0,112289-38-0,135202-48-1,148888-66-8,71696-32-7
1,2-anhydro-3,4,6-tri-O-benzyl-β-D-mannopyranose

: 136824-11-8
methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With bis(4-fluorophenyl)(hydroxy)borane; In acetonitrile; at 0 ℃; for 4h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.6b00926

Reference yield: 92.0%

: 138181-80-3
((2R,3S,4S,5R,6R)-2-Benzenesulfinyl-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-dimethyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-silane

: 136824-11-8
methyl 3,4,6-tri-O-benzyl-β-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With 2,6-di-tert-butyl-pyridine; trifluoromethylsulfonic anhydride; In diethyl ether; dichloromethane; at -100 ℃;
DOI:10.1021/ja9532291