4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide

Base Information

• Chemical Name: 4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide
• CAS No.: 64692-80-4
• Molecular Formula: C₁₄H₂₀N₂O₂S
• Molecular Weight: 280.391
• Mol file: 64692-80-4.mol

Synonyms:4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide

Chemical Property of 4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide

Chemical Property:

Purity/Quality:

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Technology Process of 4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide

There total 1 articles about 4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1-methylcyclohexan-4-one (589-92-4) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide (64692-80-4)

Guidance literature:

In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.orglett.9b03119

Reference yield: 83.0%

4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide (64692-80-4) + benzalacetophenone (94-41-7) → C22H24N2O

Guidance literature:

With caesium carbonate; In acetonitrile; at 110 ℃; for 4h; Inert atmosphere;

DOI:10.1055/s-0034-1379616

Reference yield: 20.2%

4-methyl-N’-(4-methylcyclohexylidene)benzenesulfonohydrazide (64692-80-4) + 7-chloroimidazo[1,5-a]pyridine-5-carbaldehyde → (7-chloroimidazo [1,5-a]pyridin-5-yl)(4-methylcyclohexyl)methanone

Guidance literature:

With caesium carbonate; In 1,4-dioxane; at 110 ℃; Inert atmosphere;

upstream raw materials:

1-methylcyclohexan-4-one

toluene-4-sulfonic acid hydrazide