Technology Process of C19H20O5
There total 7 articles about C19H20O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate / acetone / 15 h / Reflux
2.1: water; lithium hydroxide monohydrate / tetrahydrofuran; methanol / 15 h / -5 - 20 °C
2.2: pH 2 - 3
3.1: PPA / chlorobenzene / 15 h / 80 °C
4.1: bromine / diethyl ether / 2 h
5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
5.2: 0.5 h / -78 - 0 °C
6.1: potassium fluoride / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 15 h / Reflux
7.1: sodium hydroxide; water / 20 °C
With
potassium fluoride; lithium hydroxide monohydrate; water; bromine; potassium carbonate; sodium hydroxide; lithium hexamethyldisilazane;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; chlorobenzene; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine / diethyl ether / 2 h
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
2.2: 0.5 h / -78 - 0 °C
3.1: potassium fluoride / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 15 h / Reflux
4.1: sodium hydroxide; water / 20 °C
With
potassium fluoride; water; bromine; sodium hydroxide; lithium hexamethyldisilazane;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; diethyl ether;