<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

Base Information

• Chemical Name: <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin
• CAS No.: 133092-71-4
• Molecular Formula: C₂₂H₃₃NO₄
• Molecular Weight: 375.508

Synonyms:<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

Chemical Property of <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

Chemical Property:

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Technology Process of <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

There total 1 articles about <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-α-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzeneacetonitrile → <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin (133092-71-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;

DOI:10.1007/BF00813211

Reference yield: 95.0%

<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin (133092-71-4) → <2S-(2α,3aα,4α,7α,7aα)>-2,3,3a,4,5,6,7,7a-Octahydro-2-methoxy-7,8,8-trimethyl-4,7-methanobenzofuran (81925-10-2) + (R)-α-(Aminomethyl)-2,5-dimethoxybenzolmethanol-hydrochlorid

Guidance literature:

With hydrogenchloride; In methanol; diethyl ether;

DOI:10.1007/BF00813211

Reference yield: 85.0%

tert-butyl N-{2-[(2,5-dioxopyrrolidin-1-yl)oxy]-2-oxoethyl}carbamate (3392-07-2) + <2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin (133092-71-4) → <2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid (133163-24-3)

Guidance literature:

In tetrahydrofuran; for 0.25h; Ambient temperature;

DOI:10.1007/BF00807429

Downstream raw materials:

<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

<2S-(2α,3aα,4α,7α,7aα)>-2,3,3a,4,5,6,7,7a-Octahydro-2-methoxy-7,8,8-trimethyl-4,7-methanobenzofuran

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