4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

Base Information

Chemical Name:4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate
CAS No.:1449428-95-8
Molecular Formula:C₃₀H₂₈Cl₂N₄O₈S₂
Molecular Weight:707.612
Hs Code.:

Synonyms:4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

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Chemical Property of 4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

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Technology Process of 4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

There total 9 articles about 4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 67727-64-4
3,4-diacetoxybenzaldehyde

: 1449428-77-6
ClH*C₁₉H₁₈Cl₂N₄O₄S₂

: 1449428-95-8
4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.ejmech.2013.05.013

Reference yield:

: 2,4-dichloro-5-(morpholinosulfonyl)benzoyl chloride

: 1449428-95-8
4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 20 °C

2: dichloromethane / 2 h / 20 °C / Acidic conditions

3: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C

With pyridine; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2013.05.013

Reference yield:

: 150986-83-7
2-amino-3-cyano-4,7-dihydro-5H-thieno[2,3-c]pyridine-6-carboxylic acid tert-butyl ester

: 1449428-95-8
4-((3-cyano-2-(2,4-dichloro-5-(morpholinosulfonyl)benzamido)-4,5-dihydrothieno[2,3-c]pyridin-6(7H)-yl)methyl)-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 20 °C

2: dichloromethane / 2 h / 20 °C / Acidic conditions

3: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C

With pyridine; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2013.05.013