methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Base Information

Chemical Name:methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester
CAS No.:209546-58-7
Molecular Formula:C₁₉H₃₀N₂O₄
Molecular Weight:350.458
Hs Code.:

methyl-propyl-carbamic acid 3-(2-<i>tert</i>-butoxycarbonylamino-propyl)-phenyl ester

Synonyms:methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

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Chemical Property of methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

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Technology Process of methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

There total 3 articles about methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51493-02-8
N-methyl-N-n-propylcarbamoyl chloride

: 1027468-74-1
tert-butyl [(1R,S)-2-(3-hydroxyphenyl)-1-methylethyl]-carbamate

: 209546-58-7
methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Guidance literature:: With sodium hydride; In acetonitrile; at 20 ℃; for 6h;
DOI:10.1021/jm020120c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 209546-58-7
methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaHCO₃ / dioxane / 4 h / 20 °C

2: NaH / acetonitrile / 6 h / 20 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jm020120c

Reference yield:

: 1075-61-2,18840-47-6
Desoxy metaraminol

: 209546-58-7
methyl-propyl-carbamic acid 3-(2-tert-butoxycarbonylamino-propyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaHCO₃ / dioxane / 4 h / 20 °C

2: NaH / acetonitrile / 6 h / 20 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jm020120c