C₁₉H₂₇NO₆

Base Information

• Chemical Name: C₁₉H₂₇NO₆
• CAS No.: 1469300-34-2
• Molecular Formula: C₁₉H₂₇NO₆
• Molecular Weight: 365.426
• Mol file: 1469300-34-2.mol

Synonyms:C₁₉H₂₇NO₆

Chemical Property of C₁₉H₂₇NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₇NO₆

There total 3 articles about C₁₉H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

di-tert-butyl dicarbonate (24424-99-5) + C14H17N3O4 (1469300-42-2) → C19H27NO6 (1469300-34-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 6h; under 760.051 Torr;

DOI:10.1002/anie.201304239

Reference yield:

C13H17N3O3 → C19H27NO6 (1469300-34-2)

Guidance literature:

Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / acetonitrile / 0.17 h / 0 °C / Inert atmosphere

2: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr

With palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; acetyl chloride; In ethyl acetate; acetonitrile;

DOI:10.1002/anie.201304239

Reference yield:

C13H14N4O2 (1469300-41-1) → C19H27NO6 (1469300-34-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; acetyl chloride; In ethyl acetate;

DOI:10.1002/anie.201304239

upstream raw materials:

di-tert-butyl dicarbonate

C₁₄H₁₇N₃O₄

C₁₃H₁₄N₄O₂

Downstream raw materials:

C₂₅H₃₅N₅O₈

C₄₄H₅₈N₁₀O₁₃

C₁₈H₂₅NO₆

C₂₀H₂₇N₅O₆