4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

Base Information

Chemical Name:4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide
CAS No.:1361226-32-5
Molecular Formula:C₂₆H₃₆N₄O₂S
Molecular Weight:468.663
Hs Code.:

Synonyms:4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

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Chemical Property of 4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

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Technology Process of 4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

There total 7 articles about 4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1361226-31-4
5-(dimethylamino)-N-(4-(methylamino)phenyl)pentanamide

: 540-72-7
sodium thiocyanide

: 1710-98-1
p-tert-butyl benzoyl chloride

: 1361226-32-5
4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

Guidance literature:: sodium thiocyanide; p-tert-butyl benzoyl chloride; In acetone; at 20 ℃; for 18h;

5-(dimethylamino)-N-(4-(methylamino)phenyl)pentanamide; In acetone; at 20 ℃; for 7h;
DOI:10.1016/j.bmc.2012.01.001

Reference yield:

: 1361226-29-0
C₂₀H₂₃BrN₂O₃

: 1361226-32-5
4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane; water / 20 h / 20 °C

2.1: hydrogen bromide; acetic acid / 1 h / 20 °C

3.1: acetone / 18 h / 20 °C

3.2: 7 h / 20 °C

With hydrogen bromide; acetic acid; In dichloromethane; water; acetone;
DOI:10.1016/j.bmc.2012.01.001

Reference yield:

: 1361226-30-3
C₂₂H₂₉N₃O₃

: 1361226-32-5
4-(tert-butyl)-N-((4-(5-(dimethylamino)pentanamido)phenyl)(methyl)carbamothioyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide; acetic acid / 1 h / 20 °C

2.1: acetone / 18 h / 20 °C

2.2: 7 h / 20 °C

With hydrogen bromide; acetic acid; In acetone;
DOI:10.1016/j.bmc.2012.01.001