{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

Base Information

Chemical Name:{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}
CAS No.:150724-82-6
Molecular Formula:C₅₄H₄₂N₂O₂P₂Rh₂S₄
Molecular Weight:1146.96
Hs Code.:

Synonyms:{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

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Chemical Property of {bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

Chemical Property:

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Technology Process of {bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

There total 3 articles about {bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 150724-80-4
{(μ-6-methylbenzothiazole-2-thiolato)(COD)rhodium}

: 150724-82-6
{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

Guidance literature:: With CO; P(C₆H₅)3; In dichloromethane; under N2; CO is bubbled through a soln. of starting complex in CH2Cl2 for 20 min; a soln. of the phosphine in CH2Cl2 is added; soln. is evapd., addn. of hexane, filtration, washed, dried under vac., elem. anal.;
DOI:10.1016/0022-328X(93)80403-X

Reference yield:

: [Rh(μ-OMe)(1,5-cyclooctadiene)]2

: 150724-82-6
{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: CO; P(C₆H₅)3 / dichloromethane

With CO; P(C₆H₅)3; In dichloromethane;
DOI:10.1016/0022-328X(93)80403-X

Reference yield:

: 2268-79-3
2-mercapto-6-methylbenzothiazole

: 150724-82-6
{bis(μ-6-methylbenzothiazole-2-thiolato)dicarbonylbis(triphenylphosphine)dirhodium}

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: CO; P(C₆H₅)3 / dichloromethane

With CO; P(C₆H₅)3; In dichloromethane;
DOI:10.1016/0022-328X(93)80403-X