2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Base Information

Chemical Name:2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?
CAS No.:1428847-62-4
Molecular Formula:C₁₃H₁₆N₂O₈S
Molecular Weight:360.345
Hs Code.:

Synonyms:2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

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Chemical Property of 2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

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Technology Process of 2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

There total 6 articles about 2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1428847-61-3
2-(benzyloxy)-2-oxoethyl 3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoate

: 1428847-62-4
2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; for 0.5h; under 1810.07 Torr;

Reference yield:

: 2840-26-8
3-amino-4-methoxybenzoic acid

: 1428847-62-4
2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

2: pyridine / 1 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

4: 5%-palladium/activated carbon; hydrogen / methanol; chloroform / 0.5 h / 1551.49 Torr

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 20 °C

6: 5%-palladium/activated carbon; hydrogen / methanol / 0.5 h / 1810.07 Torr

With pyridine; dmap; 5%-palladium/activated carbon; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 167993-22-8
benzyl 3-amino-4-methoxybenzoate

: 1428847-62-4
2-(3-(N-(2-amino-2-oxoethyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 1 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: 5%-palladium/activated carbon; hydrogen / methanol; chloroform / 0.5 h / 1551.49 Torr

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 20 °C

5: 5%-palladium/activated carbon; hydrogen / methanol / 0.5 h / 1810.07 Torr

With pyridine; dmap; 5%-palladium/activated carbon; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; chloroform; N,N-dimethyl-formamide;