N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

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Chemical Name:N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine
CAS No.:1345853-09-9
Molecular Formula:C₄₂H₃₁FN₂
Molecular Weight:582.72
Hs Code.:

Synonyms:N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

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Chemical Property of N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

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Technology Process of N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

There total 4 articles about N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.2%

: 1257954-42-9
4-(bis(4-(2-phenylethynyl)phenyl)amino)benzaldehyde

: 140-75-0
para-fluorobenzylamine

: 1345853-09-9
N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

Guidance literature:: 4-(bis(4-(2-phenylethynyl)phenyl)amino)benzaldehyde; para-fluorobenzylamine; In tetrahydrofuran; ethanol; at 80 ℃; for 24h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1007/s10895-010-0677-2

Reference yield:

: 808758-81-8
4-[bis-(4-iodophenyl)amino]benzaldehyde

: 1345853-09-9
N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / 10 h / 80 °C / Inert atmosphere

2.1: tetrahydrofuran; ethanol / 24 h / 80 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; 1.1: Sonogashira coupling;
DOI:10.1007/s10895-010-0677-2

Reference yield:

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 1345853-09-9
N-(4-((4-fluorobenzylamino)methyl)phenyl)-4-(2-phenylethynyl)-N-(4-(2-phenylethynyl)phenyl)benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium iodate; acetic acid; potassium iodide / water / 4 h / 80 °C

2.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / 10 h / 80 °C / Inert atmosphere

3.1: tetrahydrofuran; ethanol / 24 h / 80 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

With potassium iodate; copper(l) iodide; palladium diacetate; acetic acid; triethylamine; triphenylphosphine; potassium iodide; In tetrahydrofuran; ethanol; water; 2.1: Sonogashira coupling;
DOI:10.1007/s10895-010-0677-2