4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

Base Information

Chemical Name:4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine
CAS No.:1313588-84-9
Molecular Formula:C₄₂H₄₃ClN₂O₁₈S
Molecular Weight:931.325
Hs Code.:

Synonyms:4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

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Chemical Property of 4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

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Technology Process of 4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

There total 3 articles about 4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 120238-95-1
4-(4-chlorophenyl)-2-oxo-6-(thien-2-yl)-1,2-dihydropyridine-3-carbonitrile

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 1313588-84-9
4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

Guidance literature:: 4-(4-chlorophenyl)-2-oxo-6-(thien-2-yl)-1,2-dihydropyridine-3-carbonitrile; With potassium carbonate; In N,N-dimethyl-formamide; acetone; for 1h;

2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide; In N,N-dimethyl-formamide; acetone; Reflux;
DOI:10.1016/j.ejmech.2011.04.019

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1313588-84-9
4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide

2.1: ammonium acetate / ethanol / 10 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide; acetone / 1 h

3.2: Reflux

With ammonium acetate; potassium carbonate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2011.04.019

Reference yield:

: 88-15-3,97511-16-5
2-Acetylthiophene

: 1313588-84-9
4-(4-chlorophenyl)-2-[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyloxy]-6-(thien-2-yl)-3-cyanopyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide

2.1: ammonium acetate / ethanol / 10 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide; acetone / 1 h

3.2: Reflux

With ammonium acetate; potassium carbonate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2011.04.019