C₂₇H₄₆O₆Si

Base Information

Chemical Name:C₂₇H₄₆O₆Si
CAS No.:1279710-30-3
Molecular Formula:C₂₇H₄₆O₆Si
Molecular Weight:494.744
Hs Code.:

C<sub>27</sub>H<sub>46</sub>O<sub>6</sub>Si

Synonyms:C₂₇H₄₆O₆Si

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Chemical Property of C₂₇H₄₆O₆Si

Chemical Property:

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Technology Process of C₂₇H₄₆O₆Si

There total 8 articles about C₂₇H₄₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279710-29-0
C₂₁H₃₂O₆

: 93297-61-1
TBSOTf

: 1279710-30-3
C₂₇H₄₆O₆Si

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃;
DOI:10.1016/j.tetlet.2011.01.042

Reference yield:

: 1279710-25-6
C₂₈H₅₀O₄Si₂

: 1279710-30-3
C₂₇H₄₆O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / -35 - -25 °C

2: hydrogen / benzene / 24 °C

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / -25 °C / Molecular sieve

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 °C

5: camphor-10-sulfonic acid / dichloromethane / 0 °C

6: pyridine / 0 °C

7: 2,6-dimethylpyridine / dichloromethane / 0 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; In tetrahydrofuran; dichloromethane; benzene; 3: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.01.042

Reference yield:

: 1279710-26-7
C₂₂H₃₆O₄Si

: 1279710-30-3
C₂₇H₄₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen / benzene / 24 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / -25 °C / Molecular sieve

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 °C

4: camphor-10-sulfonic acid / dichloromethane / 0 °C

5: pyridine / 0 °C

6: 2,6-dimethylpyridine / dichloromethane / 0 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; In tetrahydrofuran; dichloromethane; benzene; 2: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.01.042