N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

Base Information

Chemical Name:N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide
CAS No.:129872-19-1
Molecular Formula:C₂₇H₂₉NO
Molecular Weight:383.533
Hs Code.:

Synonyms:N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

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Technology Process of N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

There total 5 articles about N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 118495-26-4
2-methyl-2-cyclopentene-1-carboxylic acid chloride

: 129872-14-6,129872-15-7
(3-cyclopropyl-2-butenylidene)(diphenylmethyl)amine

: 129872-19-1
N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: With N,N-diethylaniline; In toluene; 1) -78 deg C, 2) warming up to room temperature overnight;
DOI:10.1021/jo00002a029

Reference yield:

: 25662-31-1
methyl 2-methyl-2-cyclopentene-1-carboxylate

: 129872-19-1
N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / KOH / methanol; H₂O / 4 h / Heating

2: oxalyl chloride / benzene / 2 h

3: 71 percent / N,N-diethylaniline / toluene / 1) -78 deg C, 2) warming up to room temperature overnight

With potassium hydroxide; oxalyl dichloride; N,N-diethylaniline; In methanol; water; toluene; benzene;
DOI:10.1021/jo00002a029

Reference yield:

: 872-77-5
3-cyclopropylbut-2-enal

: 129872-19-1
N-(diphenylmethyl)-N-(3'-cyclopropyl-1',3'-butadienyl)-2-methyl-2-cyclopentene-1-carboxylic amide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0.5 h, 0 deg C, then 1 h, room temperature

2: 71 percent / N,N-diethylaniline / toluene / 1) -78 deg C, 2) warming up to room temperature overnight

With N,N-diethylaniline; In diethyl ether; toluene;
DOI:10.1021/jo00002a029