2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

Base Information

Chemical Name:2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan
CAS No.:111075-25-3
Molecular Formula:C₂₇H₃₂O₃
Molecular Weight:404.549
Hs Code.:

Synonyms:2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

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Chemical Property of 2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

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Technology Process of 2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

There total 4 articles about 2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61227-48-3
[(3-methoxyphenyl)methyl]propanedioic acid diethyl ester

: 111075-25-3
2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

Guidance literature:: Multi-step reaction with 4 steps

1: 71.5 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

2: 82 percent / THF, HMPA, sodium hydride / paraffin / 7 h / Ambient temperature

3: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

4: 1.) phenyllithium / 1.) THF, ether, 10 min, -60 deg C, 2.) THF, ether, 15 min, -30 deg C

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sodium hydride; phenyllithium; pyridinium chlorochromate; In diethyl ether; dichloromethane; paraffin;
DOI:10.1002/recl.19861051206

Reference yield:

: 77756-13-9
2-<(3-methoxyphenyl)methyl>-1,3-propanediol

: 111075-25-3
2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / THF, HMPA, sodium hydride / paraffin / 7 h / Ambient temperature

2: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

3: 1.) phenyllithium / 1.) THF, ether, 10 min, -60 deg C, 2.) THF, ether, 15 min, -30 deg C

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; phenyllithium; pyridinium chlorochromate; In dichloromethane; paraffin;
DOI:10.1002/recl.19861051206

Reference yield:

: 111075-23-1
3-methoxy-β-(phenylmethoxymethyl)benzenepropanol

: 111075-25-3
2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

2: 1.) phenyllithium / 1.) THF, ether, 10 min, -60 deg C, 2.) THF, ether, 15 min, -30 deg C

With phenyllithium; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/recl.19861051206