(1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

Base Information

Chemical Name:(1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol
CAS No.:1397855-10-5
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:(1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

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Technology Process of (1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

There total 1 articles about (1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1397854-98-6
(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-phenylethylamino-5,6-dideoxy-1,2-O-isopropyl-idene]-α-D-gluco-heptofuranuronate

: 1397855-10-5
(1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1080/00397911.2011.587079

Reference yield: 64.0%

: 1397855-10-5
(1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol

: 3-O-benzyl-4-N-phenylethyl azetidine-1,2-O-isopropylidene-β-L-idofuranose

Guidance literature:: (1R,2R,3S,4R,5S)-[3-O-benzyl-5,6-dideoxy-5-phenylethylamino-1,2-Oisopropylidene-1,4-pento-uranos-4-yl]-β-L-ido-heptanol; With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With triphenylphosphine; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1080/00397911.2011.587079