(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

Base Information

Chemical Name:(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide
CAS No.:184034-97-7
Molecular Formula:C₁₆H₂₄N₂O
Molecular Weight:260.379
Hs Code.:

Synonyms:(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

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Chemical Property of (1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

Chemical Property:

Purity/Quality:

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Technology Process of (1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

There total 1 articles about (1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (αS,1RS,2RS)-2-Methyl-1-(α-methylbenzylamino)cyclohexanecarbonitrile

: 184034-97-7
(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184034-98-8
(1S,2S)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184035-00-5
(1R,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184034-99-9
(1R,2S)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

Guidance literature:: With sulfuric acid; In hexane; for 102h; Yield given. Yields of byproduct given;
DOI:10.1002/jlac.199619961126

Reference yield:

: 184034-97-7
(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184035-01-6
(1S,2R)-1-Amino-2-methyl-cyclohexanecarboxylic acid amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 45 ℃; for 24h; under 3750.3 Torr;
DOI:10.1002/jlac.199619961126

Reference yield:

: 184034-97-7
(1S,2R)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: (1S,2R)-1-Amino-2-methyl-cyclohexanecarboxylic acid; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 24 h / 45 °C / 3750.3 Torr

2: 99 percent / conc. aq. HCl / 1.) r.t., 2 h, 2.) 80 deg C, 10 h

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1002/jlac.199619961126