2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester

Base Information

• Chemical Name: 2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester
• CAS No.: 380356-20-7
• Molecular Formula: C₄₄H₄₁O₁₁P
• Molecular Weight: 776.777

Synonyms:2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester

Chemical Property of 2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester

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Technology Process of 2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester

There total 1 articles about 2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ⁵-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

dimethyl 2‐(benzo[d][1,3]dioxol‐5‐ylmethylene)malonate (54022-32-1) + (3aR,8aR)-2,2-dimethyl-4,4,8,8-tetraphenylperhydro-6λ5-[1,3]dioxolo-[4,5-e][1,3,2]dioxaphosphepin-6-one (329363-38-4) → 2-[(S)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ5-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester (380356-20-7) + 2-[(R)-Benzo[1,3]dioxol-5-yl-((3aR,8aR)-2,2-dimethyl-6-oxo-4,4,8,8-tetraphenyl-tetrahydro-6λ5-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)-methyl]-malonic acid dimethyl ester

Guidance literature:

With iron(III) oxide; potassium hydroxide; water; In dichloromethane; at 20 ℃; for 18h;

DOI:10.1021/ol016591v

upstream raw materials:

dimethyl 2‐(benzo[d][1,3]dioxol‐5‐ylmethylene)malonate

(3aR,8aR)-2,2-dimethyl-4,4,8,8-tetraphenylperhydro-6λ⁵-[1,3]dioxolo-[4,5-e][1,3,2]dioxaphosphepin-6-one

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