3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester

Base Information

• Chemical Name: 3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester
• CAS No.: 1043894-02-5
• Molecular Formula: C₂₃H₂₈N₂O₄
• Molecular Weight: 396.486

Synonyms:3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester

Chemical Property of 3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester

Chemical Property:

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Technology Process of 3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester

There total 1 articles about 3-(tricyclo[3.3.1.1^3,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N-[aminocarbonyl(tricyclo[3.3.1.13,7]dec-1-yl)methyl]glycine ethyl ester (1043893-92-0) + Benzyl bromoacetate (5437-45-6) → 3-(tricyclo[3.3.1.13,7]dec-1-yl)-2,6-dioxopiperazine-1-acetic acid benzyl ester (1043894-02-5)

Guidance literature:

N-[aminocarbonyl(tricyclo[3.3.1.1^3,7]dec-1-yl)methyl]glycine ethyl ester; With potassium hexamethylsilazane; In tetrahydrofuran; at 20 ℃; for 1h;

Benzyl bromoacetate; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Further stages.;

DOI:10.1016/j.tet.2008.05.005

upstream raw materials:

N-[aminocarbonyl(tricyclo[3.3.1.1^3,7]dec-1-yl)methyl]glycine ethyl ester

Benzyl bromoacetate

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