patellamide B

Base Information

Chemical Name:patellamide B
CAS No.:101914-82-3
Molecular Formula:C₃₈H₄₈N₈O₆S₂
Molecular Weight:776.981
Hs Code.:

Synonyms:patellamide B

Suppliers and Price of patellamide B

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of patellamide B

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of patellamide B

There total 36 articles about patellamide B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 101924-78-1
(4S,7S,10R,17S,20S,23R)-10-Benzyl-20-sec-butyl-4,17-bis-((S)-1-hydroxy-ethyl)-7-isobutyl-23-methyl-12,25-dithia-3,6,9,16,19,22,27,28-octaaza-tricyclo[22.2.1.1^11,14]octacosa-1⁽²⁶⁾,11⁽²⁸⁾,13,24⁽²⁷⁾-tetraene-2,5,8,15,18,21-hexaone

: 101914-82-3
patellamide B

Guidance literature:: With thionyl chloride; at 4 ℃; for 53h;
DOI:10.1016/S0040-4039(00)98890-7

Reference yield: 50.0%

: C₄₄H₄₉F₅N₈O₇S₂

: 101914-82-3
patellamide B

Guidance literature:: With 2-pyrrolidinopyridine; In 1,4-dioxane; for 3h;
DOI:10.1016/S0040-4039(00)98736-7

Reference yield:

: 101817-28-1
2-((S)-1-Hydroxy-ethyl)-thiazole-4-carbonitrile

: 101914-82-3
patellamide B

Guidance literature:: Multi-step reaction with 8 steps

1: 91 percent / NaOEt / 24 h / Ambient temperature

2: 60 percent / CH₂Cl₂ / 24 h / Ambient temperature

3: 70 percent / diethylazodicarboxylate, P(Ph)3, HN₃ / 1 h / Ambient temperature

4: Pd, H₂

5: 40 percent / DCCD, CuCl₂ / 72 h / 0 deg C to room temperature

6: 1.) NaOH, 2.) DCCD / 1.) dioxane, water, romm temperature, 5 h, 2.) 1 d

7: 95 percent / CF₃COOH / 0.42 h / 0 °C

8: 50 percent / pyrrolidinopyridine / dioxane / 3 h

With sodium hydroxide; 2-pyrrolidinopyridine; tris-(2-chloro-ethyl)-amine; hydrogen; sodium ethanolate; palladium; dicyclohexyl-carbodiimide; triphenylphosphine; trifluoroacetic acid; copper dichloride; diethylazodicarboxylate; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0040-4039(00)98736-7