((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

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Chemical Name:((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}
CAS No.:154827-02-8
Molecular Formula:AlCl₄*C₆₁H₆₃NiP₄Si₂
Molecular Weight:1203.72
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3P)3NiPC(Si(CH<sub>3</sub>)3)2<sup>(1+)</sup>*AlCl<sub>4</sub><sup>(1-)</sup>={((C<sub>6</sub>H<sub>5</sub>)3P)3NiPC(Si(CH<sub>3</sub>)3)2}{AlCl<sub>4</sub>}

Synonyms:((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

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Chemical Property of ((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

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Technology Process of ((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

There total 2 articles about ((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 12151-13-2
cycloocta-1,5-dienebis(triphenylphosphine)nickel⁽⁰⁾

: (C₆H₅)3PPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={(C₆H₅)3PPC(Si(CH₃)3)2}{AlCl₄}

: 154827-02-8
((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

Guidance literature:: In toluene; byproducts: cyclooctadiene; to a suspn. of the P-compd. in toluene was added a soln. of the Ni complex at 0°C, warmed to room temp.; separation of the solvent phase, cooling of the remaining oil to 0°C;
DOI:10.1021/ja00084a088

Reference yield:

: 79454-85-6
[bis(trimethylsilyl)methylene]chlorophosphane

: 154827-02-8
((C₆H₅)3P)3NiPC(Si(CH₃)3)2⁽¹⁺⁾*AlCl₄^(1-)={((C₆H₅)3P)3NiPC(Si(CH₃)3)2}{AlCl₄}

Guidance literature:: Multi-step reaction with 2 steps

1: triphenyl phosphine / toluene

2: toluene

With triphenyl phosphine; In toluene;
DOI:10.1021/ja00084a088