Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

Base Information

Chemical Name:Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester
CAS No.:181627-15-6
Molecular Formula:C₁₆H₂₂NO₇P
Molecular Weight:371.327
Hs Code.:

Synonyms:Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

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Chemical Property of Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

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Technology Process of Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

There total 1 articles about Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 504-61-0,542-72-3
(E)-but-2-enol

: 89525-07-5
(+/-)-2-<(benzyloxycarbonyl)amino>-2-(dimethoxyphosphinyl)acetic acid

: 181627-15-6
Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In various solvent(s);
DOI:10.1016/0040-4039(96)01104-5

Reference yield: 74.0%

: 122-78-1
phenylacetaldehyde

: 181627-15-6
Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

: (E)-2-Benzyloxycarbonylamino-4-phenyl-but-2-enoic acid (E)-but-2-enyl ester

: (Z)-2-Benzyloxycarbonylamino-4-phenyl-but-2-enoic acid (E)-but-2-enyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 20h; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1016/0040-4039(96)01104-5

Reference yield:

: 122-78-1
phenylacetaldehyde

: 181627-15-6
Benzyloxycarbonylamino-(dimethoxy-phosphoryl)-acetic acid (E)-but-2-enyl ester

: (2S,3R)-2-Benzyloxycarbonylamino-3-methyl-2-((Z)-styryl)-pent-4-enoic acid

: (2S,3R)-2-Benzyloxycarbonylamino-3-methyl-2-((E)-styryl)-pent-4-enoic acid

: (2S,3S)-2-Benzyloxycarbonylamino-3-methyl-2-((E)-styryl)-pent-4-enoic acid

Guidance literature:: With oxonium; 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) chloride; lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) CH₂Cl₂, 20 h, r.t.;
DOI:10.1016/0040-4039(96)01104-5