1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

Base Information

Chemical Name:1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide
CAS No.:525552-18-5
Molecular Formula:C₁₈H₃₄O₅
Molecular Weight:330.465
Hs Code.:

Synonyms:1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

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Chemical Property of 1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

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Technology Process of 1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

There total 3 articles about 1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 525552-16-3
C₂₄H₄₈O₅Si

: 525552-18-5
1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4020(02)01556-9

Reference yield:

: 5212-80-6
5-methylhex-5-en-1-ol

: 525552-18-5
1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II) / CH₂Cl₂ / 20 °C

2: 60 percent / O₃ / CH₂Cl₂ / -70 °C

3: 15 percent / Ag₂O / CH₂Cl₂ / 20 °C

4: 63 percent / KF; 18-crown-6 / tetrahydrofuran / 20 °C

With potassium fluoride; 18-crown-6 ether; (1-morpholinocarbamoyl-4,4-Me₂-1,3-pentanedionato)2Co(II); ozone; silver(l) oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(02)01556-9

Reference yield:

: 525552-14-1
C₁₉H₄₀O₅Si

: 525552-18-5
1,1-dimethyl-5-[1-(3-methyl-but-3-enylperoxy)-cyclohexyloxy]-pentyl hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent / Ag₂O / CH₂Cl₂ / 20 °C

2: 63 percent / KF; 18-crown-6 / tetrahydrofuran / 20 °C

With potassium fluoride; 18-crown-6 ether; silver(l) oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(02)01556-9