3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium

Base Information

• Chemical Name: 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium
• CAS No.: 701980-18-9
• Molecular Formula: C₃₀H₂₉IN₃O₄
• Molecular Weight: 622.482

Synonyms:3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium

Chemical Property of 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium

Chemical Property:

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Technology Process of 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium

There total 2 articles about 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,3-Diiodopropane (627-31-6) + 3,8-bis[(allyloxycarbonyl)amino]-6-phenylphenanthridine (666841-56-1) → 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium (701980-18-9)

Guidance literature:

In tetrahydrofuran; at 65 ℃; for 216h;

DOI:10.1002/anie.200353153

Reference yield:

3,8-diamino-6-phenylphenanthridine (52009-64-0) → 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium (701980-18-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂ / 24 h / 20 °C

2: 82 percent / tetrahydrofuran / 216 h / 65 °C

In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.200353153

Reference yield: 89.0%

(2S,3S)-3-amino-4-{4,4’-dimethoxytrityloxy}butan-2-ol (956092-70-9) + 3,8-bis-allyloxycarbonylamino-5-(3-iodo-propyl)-6-phenyl-phenanthridinium (701980-18-9) → C55H57N4O8(1+) (956092-71-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 120h;

DOI:10.1055/s-2007-984899

upstream raw materials:

1,3-Diiodopropane

3,8-bis[(allyloxycarbonyl)amino]-6-phenylphenanthridine

3,8-diamino-6-phenylphenanthridine

Downstream raw materials:

C₅₅H₅₇N₄O₈⁽¹⁺⁾

C₄₇H₄₉N₄O₄⁽¹⁺⁾

C₅₃H₄₆F₉N₄O₇⁽¹⁺⁾

3,8-diamino-5-(3-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-hydroxy-propylamino}-propyl)-6-phenyl-phenanthridinium

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