benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:862537-80-2
Molecular Formula:C₂₇H₂₅NO₆S
Molecular Weight:491.565
Hs Code.:

Synonyms:benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Chemical Property of benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Technology Process of benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

There total 5 articles about benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501416-24-6
benzoxazol-2-yl 3,4,6-tri-O-acetyl-2-O-benzyl-1-thio-β-D-glucopyranoside

: 862537-80-2
benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOMe / methanol / 0.5 h / 20 °C

2: pyridine / 2 h / Heating

With pyridine; sodium methylate; In methanol;
DOI:10.1021/jo071191s

Reference yield:

: 29741-69-3
3,4,6-tetra-O-acetyl-2-O-benzyl-α-D-glucopyranosyl bromide

: 862537-80-2
benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / acetone; toluene / 16 h / 20 °C

2: MeONa / methanol

3: DMT

With N,N-dimethyltryptamine; sodium methylate; potassium carbonate; In methanol; acetone; toluene;
DOI:10.1021/ol0273452

Reference yield:

: 2382-96-9,118090-08-7
2-sulfanyl-1,3-benzoxazole

: 862537-80-2
benzoxazol-2-yl 2-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / acetone; toluene / 16 h / 20 °C

2: MeONa / methanol

3: DMT

With N,N-dimethyltryptamine; sodium methylate; potassium carbonate; In methanol; acetone; toluene;
DOI:10.1021/ol0273452