2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide

Base Information

Chemical Name:2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide
CAS No.:144170-10-5
Molecular Formula:C₂₇H₂₈BrNO₂
Molecular Weight:478.429
Hs Code.:
Mol file:144170-10-5.mol

Synonyms:2-Bromo-5-nitroanisol;2-Brom-5-nitro-anisol;4-Bromo-3-methoxynitrobenzene;1-bromo-2-methoxy-4-nitro-benzene;Benzene,1-bromo-2-methoxy-4-nitro;2-bromo 5-nitro anisole;

Suppliers and Price of 2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide

Chemical Property:

Vapor Pressure:1.32E-13mmHg at 25°C
Boiling Point:583.6°C at 760 mmHg
Flash Point:306.7°C
PSA：41.82000
Density:1.293g/cm³
LogP:8.00840

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide

There total 4 articles about 2-bromo-N-[2,6-di(propan-2-yl)phenyl]-6,11-dihydrodibenzo[b,e]oxepine-11-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144170-68-3,144170-82-1,144170-83-2
2-bromo-6,11-dihydrodibenzoxepin-11-carboxylic acid

: 144170-10-5,144170-50-3,144170-51-4
(+/-)-2-bromo-N-(2,6-diisopropylphenyl)-6,11-dihydrodibenzoxepin-11-carboxamide

Guidance literature:

Reference yield:

: 2-bromo-11-hydroxy-6,11-dihydrodibenzoxepin

: 144170-10-5,144170-50-3,144170-51-4
(+/-)-2-bromo-N-(2,6-diisopropylphenyl)-6,11-dihydrodibenzoxepin-11-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) SOCl₂ / 1.) CH₂Cl₂, RT, 17 h, 2.) CH₂Cl₂, toluen, reflux, 2 h

2: 4.15 g / HCl-AcOH / 24 h / Heating

3: 1.) SOCl₂, 2.) NEt₃ / 1.) CH₂Cl₂, 2.) CH₂Cl₂

With hydrogenchloride; thionyl chloride; acetic acid; triethylamine;
DOI:10.1021/jm00032a014

Reference yield:

: 154775-78-7
2-bromo-6,11-dihydrodibenz[b,e]oxepin-11-carbonitrile

: 144170-10-5,144170-50-3,144170-51-4
(+/-)-2-bromo-N-(2,6-diisopropylphenyl)-6,11-dihydrodibenzoxepin-11-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4.15 g / HCl-AcOH / 24 h / Heating

2: 1.) SOCl₂, 2.) NEt₃ / 1.) CH₂Cl₂, 2.) CH₂Cl₂

With hydrogenchloride; thionyl chloride; acetic acid; triethylamine;
DOI:10.1021/jm00032a014