C₁₅H₁₄OS₂

Base Information

• Chemical Name: C₁₅H₁₄OS₂
• CAS No.: 1333203-99-8
• Molecular Formula: C₁₅H₁₄OS₂
• Molecular Weight: 274.408
• Mol file: 1333203-99-8.mol

Synonyms:C₁₅H₁₄OS₂

Chemical Property of C₁₅H₁₄OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₄OS₂

There total 4 articles about C₁₅H₁₄OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H12OS2 → C15H14OS2 (1333203-99-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201102562

Reference yield:

phenylacetaldehyde (122-78-1) → C15H14OS2 (1333203-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; (5S)-5-benzyl-2,2,3-trimethylimidazolidin-4-one; benzoic acid / water; acetonitrile / 24 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; sodium dihydrogenphosphate; (5S)-5-benzyl-2,2,3-trimethylimidazolidin-4-one; benzoic acid; In methanol; water; acetonitrile;

DOI:10.1002/anie.201102562

Reference yield:

1,3-benzodithiol-2-ylium tetrafluoroborate (57842-27-0) → C15H14OS2 (1333203-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C

2: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

With sodium tetrahydroborate; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride; In methanol; water; acetonitrile;

DOI:10.1002/adsc.201300250

upstream raw materials:

phenylacetaldehyde

1,3-benzodithiol-2-ylium tetrafluoroborate

Downstream raw materials:

(S)-2-phenyl-1-propanol

methyl (R)-(-)-4-phenylpentanoate

C₁₄H₁₈O₄

(S)-(2-iodo-1-methylethyl)benzene