Technology Process of C36H38O5
There total 4 articles about C36H38O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
Inert atmosphere;
Cooling with ice;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere; Cooling with ice
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
2.2: 0.33 h / -78 °C / Inert atmosphere
2.3: 1 h / -78 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
3.2: 2 h / 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Cooling with ice
With
1H-imidazole; n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
1.2: 0.33 h / -78 °C / Inert atmosphere
1.3: 1 h / -78 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Cooling with ice
With
n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; hexane;
DOI:10.1039/c1ob05251a