2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

Base Information

Chemical Name:2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride
CAS No.:478556-29-5
Molecular Formula:C₂₁H₁₅Cl₆CoN₃
Molecular Weight:581.081
Hs Code.:

Synonyms:2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

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Chemical Property of 2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

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Technology Process of 2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

There total 2 articles about 2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 323179-70-0
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine

: cobalt(II) chloride dihydrate

: 478556-29-5
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2019.02.002

Reference yield: 80.0%

: 323179-70-0
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 478556-29-5
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine cobalt(II) chloride

Guidance literature:: In tetrahydrofuran; ligand was added to soln. CoCl2 in THF at room temp. with stirring and stirred at room temp. for 12 h; react. mixt. was concd. and allowed to stand at room temp. for several hours, supernatant was removed, residue was washed with Et2O and dried invacuo; elem. anal.;
DOI:10.1021/om0302894