1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione

Base Information

• Chemical Name: 1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione
• CAS No.: 120154-53-2
• Molecular Formula: C₂₆H₂₁N₂O₃P
• Molecular Weight: 440.438
• Mol file: 120154-53-2.mol

Synonyms:1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione

Chemical Property of 1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione

There total 1 articles about 1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isocyanatoethene (3555-94-0) + Bestmann ylide (73818-55-0,15596-07-3) → 3-triphenylphosphorano-2,4-pyridinedione (120154-52-1) + 1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione (120154-53-2)

Guidance literature:

In benzene; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)85843-9

Reference yield: 80.0%

1-(N-ethenylcarbamoyl)-3-triphenylphosphorano-2,4-pyridinedione (120154-53-2) → 3-triphenylphosphorano-2,4-pyridinedione (120154-52-1)

Guidance literature:

In decalin; at 170 ℃; for 1h; Heating;

DOI:10.1016/S0040-4020(01)85843-9

upstream raw materials:

isocyanatoethene

Bestmann ylide

Downstream raw materials:

3-triphenylphosphorano-2,4-pyridinedione