Technology Process of C53H35N3
There total 3 articles about C53H35N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate;
In
toluene;
at 110 ℃;
for 12h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; copper(l) chloride; 1,10-Phenanthroline / dimethyl sulfoxide / 12 h / 150 °C / Inert atmosphere
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; tetrahydrofuran; water / 12 h / Inert atmosphere; Reflux
3: bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate; tri-tert-butyl phosphine / toluene / 12 h / 110 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); 1,10-Phenanthroline; tri-tert-butyl phosphine; potassium carbonate; copper(l) chloride; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate;
In
tetrahydrofuran; water; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; tetrahydrofuran; water / 12 h / Inert atmosphere; Reflux
2: bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate; tri-tert-butyl phosphine / toluene / 12 h / 110 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; potassium carbonate; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate;
In
tetrahydrofuran; water; toluene;