3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone

Base Information

• Chemical Name: 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone
• CAS No.: 126401-48-7
• Molecular Formula: C₂₁H₂₈N₂O₅
• Molecular Weight: 388.464

Synonyms:3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone

Chemical Property of 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone

Chemical Property:

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Technology Process of 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone

There total 2 articles about 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

morpholine (110-91-8,99108-56-2) + 3-Benzyl-4-((S)-4-isopropyl-2-oxo-oxazolidin-3-yl)-4-oxo-butyric acid → (S)-2-Benzyl-1-((S)-4-isopropyl-2-oxo-oxazolidin-3-yl)-4-morpholin-4-yl-butane-1,4-dione (126401-48-7) + 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone (126401-48-7)

Guidance literature:

With diethylphosphoryl cyanide; triethylamine; In tetrahydrofuran; at 0 ℃; for 2h; Yield given;

DOI:10.1248/cpb.37.2200

Reference yield:

morpholine (110-91-8,99108-56-2) + 3-Benzyl-4-((S)-4-isopropyl-2-oxo-oxazolidin-3-yl)-4-oxo-butyric acid → (S)-2-Benzyl-1-((S)-4-isopropyl-2-oxo-oxazolidin-3-yl)-4-morpholin-4-yl-butane-1,4-dione (126401-48-7) + 3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone (126401-48-7)

Guidance literature:

With diethylphosphoryl cyanide; triethylamine; In tetrahydrofuran; at 0 ℃; for 2h; Yield given;

DOI:10.1248/cpb.37.2200

Reference yield: 76.0%

3-<2-(R)-benzyl-1,4-dioxo-4-morpholinobutyl>-4-(S)-isopropyl-2-oxazolidinone (126401-48-7) → 2(R)-2-<(4-morpholinylcarbonyl)methyl>-3-phenylpropionic acid (112804-14-5)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 3h;

DOI:10.1248/cpb.37.2200

upstream raw materials:

morpholine

Downstream raw materials:

2(R)-2-<(4-morpholinylcarbonyl)methyl>-3-phenylpropionic acid

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