O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

Base Information

Chemical Name:O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate
CAS No.:1346434-65-8
Molecular Formula:C₁₉H₂₈ClN₅O₃
Molecular Weight:409.916
Hs Code.:

Synonyms:O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

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Chemical Property of O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

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Technology Process of O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

There total 4 articles about O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146292-90-2
6-azidohexan-1-ol

: 1346434-65-8
O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / tetrahydrofuran / 0.67 h / 20 °C

2: pyridine / tetrahydrofuran / 2 h / 20 °C

3: chloro-trimethyl-silane / tetrahydrofuran / 41 h / 65 °C

With pyridine; chloro-trimethyl-silane; In tetrahydrofuran;
DOI:10.1021/bc4002882

Reference yield:

: C₈H₁₂Cl₃N₃O₃

: 1346434-65-8
O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 2 h / 20 °C

2: chloro-trimethyl-silane / tetrahydrofuran / 41 h / 65 °C

With pyridine; chloro-trimethyl-silane; In tetrahydrofuran;
DOI:10.1021/bc4002882

Reference yield:

: 1346453-80-2
6-azidohexyl carbonochloridate

: 1346434-65-8
O-[6-azidohexyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h

2: chloro-trimethyl-silane / toluene / 24 h / 50 °C / Inert atmosphere

With chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jm401644v