N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane

Base Information

• Chemical Name: N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane
• CAS No.: 75956-66-0
• Molecular Formula: C₄₀H₄₉N₃O₁₅
• Molecular Weight: 811.84
• Mol file: 75956-66-0.mol

Synonyms:N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane

Chemical Property of N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane

There total 2 articles about N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methyl 2,3-dimethoxyterephthalate (75956-63-7) → N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane (75956-66-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / SOCl₂

2: NEt₃ / tetrahydrofuran / Ambient temperature

With thionyl chloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/jm00134a015

Reference yield:

N-(3-aminopropyl)-1,4-diaminobutane (124-20-9) + 2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid (75956-64-8) → N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane (75956-66-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; Yield given; Ambient temperature;

DOI:10.1021/jm00134a015

Reference yield: 71.0%

N,N',N'',N'''-tris<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10-triazadecane (75956-66-0) → N,N',N'',N'''-tris(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10-triazadecane (75956-68-2)

Guidance literature:

With boron tribromide; In tetrachloromethane; dichloromethane; Ambient temperature;

DOI:10.1021/jm00134a015

upstream raw materials:

N-(3-aminopropyl)-1,4-diaminobutane

2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid

sodium methyl 2,3-dimethoxyterephthalate

Downstream raw materials:

N,N',N'',N'''-tris(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10-triazadecane