Technology Process of 2-Acetyl-7-phenyl-heptanenitrile
There total 5 articles about 2-Acetyl-7-phenyl-heptanenitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium amide;
In
diethyl ether; ammonia;
for 0.333333h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / H2, conc. sulfuric acid / 20percent Pd/C / methanol / 2585.7 Torr
2: 98.6 percent / lithium aluminum hydride / diethyl ether / 16 h / Heating
3: 99 percent / thionyl chloride / CHCl3 / 1 h / Heating
4: 98.5 percent / potassium iodide / dimethylsulfoxide
5: 72 percent / sodium amide / liquid ammonia; diethyl ether / 0.33 h
With
lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; hydrogen; sodium amide; potassium iodide;
palladium on activated charcoal;
In
methanol; diethyl ether; chloroform; ammonia; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / thionyl chloride / CHCl3 / 1 h / Heating
2: 98.5 percent / potassium iodide / dimethylsulfoxide
3: 72 percent / sodium amide / liquid ammonia; diethyl ether / 0.33 h
With
thionyl chloride; sodium amide; potassium iodide;
In
diethyl ether; chloroform; ammonia; dimethyl sulfoxide;
