3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

Base Information

Chemical Name:3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one
CAS No.:174485-35-9
Molecular Formula:C₂₇H₃₅NO₃
Molecular Weight:421.58
Hs Code.:

Synonyms:3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

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Chemical Property of 3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

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Technology Process of 3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

There total 10 articles about 3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174485-34-8
3-[2,2-Dimethyl-1-(3-nitro-phenyl)-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

: 174485-35-9
3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 760 Torr;
DOI:10.1021/jm9802158

Reference yield:

: 29898-25-7
1-phenylhexan-3-one

: 174485-35-9
3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH, 2.) n-BuLi, 3.) 6 N HCl

2: aq. NaOH / methanol

3: AlCl₃ / tetrahydrofuran / 2 h / Ambient temperature

4: 1.) Zn, 2.) CuCN, LiCl

5: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

With hydrogenchloride; sodium hydroxide; n-butyllithium; aluminium trichloride; hydrogen; sodium hydride; lithium chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm9802158

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 174485-35-9
3-[1-(3-Amino-phenyl)-2,2-dimethyl-propyl]-5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / tetrahydrofuran / 2 h / Ambient temperature

2: 1.) Zn, 2.) CuCN, LiCl

3: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

With aluminium trichloride; hydrogen; lithium chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm9802158