Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate

Base Information

• Chemical Name: Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate
• CAS No.: 1179524-60-7
• Molecular Formula: C₁₂H₁₃ClNO₄S*Li
• Molecular Weight: 309.7
• Mol file: 1179524-60-7.mol

Synonyms:Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate

Chemical Property of Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate

There total 1 articles about Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-Chloro-benzenesulfonyl)-piperidine-3-carboxylic acid ethyl ester (1156725-31-3) → Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate (1179524-60-7)

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃; for 5 - 6h;

Reference yield: 20.8%

2-(3-methylphenyl)pyrrolidine (72216-05-8) + Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate (1179524-60-7) → [1-(2-Chloro-benzenesulfonyl)-piperidin-3-yl]-(2-m-tolyl-pyrrolidin-1-yl)-methanone (1179524-40-3)

Guidance literature:

2-(3-methylphenyl)pyrrolidine; Lithium 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With HATU; In N,N-dimethyl-formamide; at 20 ℃;

upstream raw materials:

1-(2-Chloro-benzenesulfonyl)-piperidine-3-carboxylic acid ethyl ester

Downstream raw materials:

[1-(2-Chloro-benzenesulfonyl)-piperidin-3-yl]-(2-m-tolyl-pyrrolidin-1-yl)-methanone