C₃₅H₃₃N₃O₄S

Base Information

Chemical Name:C₃₅H₃₃N₃O₄S
CAS No.:1338711-14-0
Molecular Formula:C₃₅H₃₃N₃O₄S
Molecular Weight:591.731
Hs Code.:

C<sub>35</sub>H<sub>33</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:C₃₅H₃₃N₃O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₃₃N₃O₄S

Chemical Property:

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Technology Process of C₃₅H₃₃N₃O₄S

There total 9 articles about C₃₅H₃₃N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1338711-05-9
C₃₅H₃₂BrN₃O₄S

: 1338711-14-0
C₃₅H₃₃N₃O₄S

Guidance literature:: With tert.-butyl lithium; In diethyl ether; pentane; at -40 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol202475r

Reference yield:

: 61-54-1
tryptamine

: 1338711-14-0
C₃₅H₃₃N₃O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene / Reflux

2.1: pyridinium perbromide hydrobromide / tetrahydrofuran; chloroform / 2.33 h / -10 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

3.2: 4 h / 0 - 20 °C

4.1: hydrazine hydrate / ethanol / Reflux

5.1: methanol / 24 h / 20 °C

6.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere

6.2: 4 h / -40 - 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 °C

8.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -40 - 20 °C / Inert atmosphere

With pyridinium perbromide hydrobromide; boron trifluoride diethyl etherate; tert.-butyl lithium; sodium hydride; hydrazine hydrate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; mineral oil; pentane;
DOI:10.1021/ol202475r

Reference yield:

: 1338711-07-1
C₁₈H₁₉BrN₂O

: 1338711-14-0
C₃₅H₃₃N₃O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / 24 h / 20 °C

2.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere

2.2: 4 h / -40 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C

4.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -40 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; tert.-butyl lithium; sodium hydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; mineral oil; pentane;
DOI:10.1021/ol202475r