Technology Process of C36H39F2N5O5
There total 6 articles about C36H39F2N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 18h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h
1.2: 2 h
1.3: pH 2
2.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 80 °C
2.2: 3 h
3.1: caesium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 4 h / 120 °C / Inert atmosphere
4.1: water; lithium hydroxide monohydrate / methanol
5.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane
6.1: hydrogen / palladium on activated charcoal / methanol / 18 h
With
1H-imidazole; lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; hydrogen; benzotriazol-1-ol; caesium carbonate; triethylamine; dicyclohexyl-carbodiimide;
tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal;
In
methanol; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 80 °C
1.2: 3 h
2.1: caesium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 4 h / 120 °C / Inert atmosphere
3.1: water; lithium hydroxide monohydrate / methanol
4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane
5.1: hydrogen / palladium on activated charcoal / methanol / 18 h
With
lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; hydrogen; benzotriazol-1-ol; caesium carbonate; triethylamine; dicyclohexyl-carbodiimide;
tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal;
In
methanol; 1,2-dimethoxyethane; dichloromethane; toluene;