1-diamantyldiphenylphosphine oxide

Base Information

• Chemical Name: 1-diamantyldiphenylphosphine oxide
• CAS No.: 1346519-76-3
• Molecular Formula: C₂₆H₂₉OP
• Molecular Weight: 388.489
• Mol file: 1346519-76-3.mol

Synonyms:1-diamantyldiphenylphosphine oxide

Chemical Property of 1-diamantyldiphenylphosphine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-diamantyldiphenylphosphine oxide

There total 2 articles about 1-diamantyldiphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-diamantyldiphenylphosphonium triflate (1346519-75-2) → 1-diamantyldiphenylphosphine oxide (1346519-76-3)

Guidance literature:

With potassium tert-butylate; dihydrogen peroxide; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;

DOI:10.1055/s-0030-1260303

Reference yield:

1-bromodiamantane (30545-17-6) → 1-diamantyldiphenylphosphine oxide (1346519-76-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,2-Dimethylbutane / 1.5 h / 0 °C / Darkness; Inert atmosphere

2: 2,2-Dimethylbutane / 2 h / 0 - 20 °C / Darkness; Inert atmosphere

3: potassium tert-butylate; dihydrogen peroxide / dichloromethane / 14 h / 20 °C / Inert atmosphere

With potassium tert-butylate; dihydrogen peroxide; In 2,2-Dimethylbutane; dichloromethane;

DOI:10.1055/s-0030-1260303

upstream raw materials:

1-diamantyldiphenylphosphonium triflate

1-bromodiamantane