5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline

Base Information

• Chemical Name: 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline
• CAS No.: 350579-07-6
• Molecular Formula: C₁₇H₂₄OSi
• Molecular Weight: 272.462
• Mol file: 350579-07-6.mol

Synonyms:5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline

Chemical Property of 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline

There total 1 articles about 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Allylchlorodimethylsilane (4028-23-3) + (+/-)-1-phenylhex-4-yn-3-ol (184577-40-0) → 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline (350579-07-6)

Guidance literature:

Grubbs catalyst first generation; In dichloromethane; for 3h; Heating;

DOI:10.1021/ol016026s

Reference yield: 70.0%

maleiimide (541-59-3,25721-74-8) + 5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline (350579-07-6) → (3aS,6R,9aS,9bS)-5,8,8-Trimethyl-6-phenethyl-4,6,8,9,9a,9b-hexahydro-3aH-7-oxa-2-aza-8-sila-cyclopenta[a]naphthalene-1,3-dione

Guidance literature:

In toluene; Heating;

DOI:10.1021/ol016026s

Reference yield:

5-isopropenyl-2,2-dimethyl-6-phenethyl-3,6-dihydro-2H-[1,2]oxasiline (350579-07-6) → (Z)-3-Isopropenyl-6-phenyl-hex-2-ene-1,4-diol

Guidance literature:

With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; at 20 ℃; for 48h;

DOI:10.1021/ol016026s

upstream raw materials:

Allylchlorodimethylsilane

(+/-)-1-phenylhex-4-yn-3-ol